Thursday, 11 August 2011

SYLLABI FOR MASTER OF SCIENCE (INDUSTRIAL CHEMISTRY) (FIRST AND SECOND SEMESTERS) OF PUNJAB UNIVERSITY, CHANDIGARH

**List of Elective subjects (ICH 1.05 and ICH 2.05)
1. Oils and Fats Technology
2. Paper Technology
3. Paints & Varnish Technology
4. Sugar & Starch Technology
5. Polymer Technology
6. Polymer Processing
7. Fertilizers
8. Food Processing
9. Industrial Electrochemistry
10. Membrane Separation Processes

SCHEME OF TEACHING AND EXAMINATION
Paper Subject Teaching Hours
per Week
Exam.
Marks
Sessional
Marks
Total
Marks
THIRD SEMESTER L T P
ICH 3.01 Industrial Pollution Control 3 1 - 100 50 150
ICH 3.02 Chemical Engineering-III 3 1 - 100 50 150
ICH 3.03 Industrial Management 3 1 - 100 50 150
ICH 3.04 Elective –II 3 1 - 100 50 150
ICH 3.05 Literature Survey, Report
Writing & Seminar
- - 3 - 100 100
Total 12 4 3 400 300 700
List of Elective subjects for ICH 3.04
1. Oils and Fats Technology
2. Paper Technology
3. Paints & Varnish Technology
4. Sugar & Starch Technology
5. Polymer Technology
6. Polymer Processing
7. Fertilizers
8. Food Processing
9. Industrial Electrochemistry
10. Membrane Separation Processes
SCHEME OF TEACHING AND EXAMINATION
Paper Subject Exam. Marks
FOURTH SEMESTER
ICH 4.01 Comprehensive Viva-voce 100
ICH 4.02 Term Paper 100
ICH 4.03 Seminar on Thesis/Industrial Training 100
ICH 4.04 *Thesis Qualifying
Total 300
*Thesis work will be based on the research work conducted in the Department on an
approved topic under the supervision of a faculty member of the Department or it can be
based on the training in an Industrial/R&D Organization of repute under joint supervision of
one supervisor from the industry and the other from the Department.
Note: No numerical marks are to be assigned to thesis work. It is either
“Accepted” or “Rejected”. Quality of work reported in the thesis can be
graded in terms of “Very Good”, “Good” or “Average”.
SYLLABUS FOR
MASTER OF SCIENCE (INDUSTRIAL CHEMISTRY)
FIRST SEMESTER
ICH 1.01 CHEMICAL ENGINEERING-I
1. Fluid Statics and fluid properties: Normal forces in fluids, Pressure Measurements,
Newtonian and non-Newtonian Fluids, Flow in Boundary Layers, Basic Equation of Fluid Flow:
Bernoulli’s Equation. (8 Hrs.)
2. Flow of Incompressible Fluids: Laminar and Turbulent flow in pipes, Velocity Distribution in
Pipes, Frictional Losses in Pipes and Fittings, Fanning’s equation, Derivation of HAGENPOISEULLI
and f=16/Re equations. (8 Hrs.)
3. Flow Measurements: Pilot tube, Orifice, Venturi, Rotameter and Notches. (4 Hrs.)
4. Fluid Machinery: Classification and Performance of Pumps, Net positive Suction Head.
(4Hrs.)
5. Size Reduction: Crushers and Grinders: jaw crusher, Gyratory Crusher, crushing rolls, roller
mill, pin mill, ball mill, Hammer mill and Fluid energy mill. Laws of crushing. (4 Hrs.)
6. Size Separation by Screening: Stationery screens, Grizzlies, Trommel and Vibrating screens.
Standard Screens, Screening Analysis-differential and cumulative. (4 Hrs.)
7. Filtration: Plate and frame filter press, continuous rotary vacuum filter, filter aids, theory of
filtration for non-compressible cakes. (4 Hrs.)
8. Fluidization: Aggregate and particulate fluidization. Ergun’s and Carman-Kozeny equations.
(4Hrs.)
Books Recommended:
1. Mc Cabe, Warren L., Smith,
Juluain C. and Harroit, Peter
: Unit Operations of Chemical Engineering, 7th Edition,
Mc Graw Hill, New York, 2005.
2. Foust, Alan S., Wenseli, Leonard
A., Clump, Curtis W., mans,
Louis and Anersen, L. Bryce
: Principles of Unit Operations, John Wiley & Sons
Inc., New York, 2nd ed, 1980.
3. Coulson, J.M. and Richardson,
J.F.
: Unit Operations (Volume 2 of Chemical Engineering)
5th ed, Elsevier, New Delhi, 2003
4. Badger, Walter L. and
Banchero, Julius T.
: Introduction to Chemical Engineering, Mc Graw-Hill,
International edition 1955.
5. Brown, C.G. : Unit Operations, CBS Publishers and Distributors,
New Delhi, 2005.
ICH 1.02 CHEMICAL TECHNOLOGY (ORGANIC)
Pulp & Paper: Raw materials, types of pulp, manufacture of paper. (5 Hrs.)
Sugar: Introduction, juice extraction, defacation, sulphonation, carbonation, concentration,
refining. (5 Hrs.)
Fermentation: Production of ethyl alcohol from molasses, citric acid and antibiotics like
pencillin. (5 Hrs.)
Oils & Fats: Extraction of oils from vegetable oils, refining of oils and fats, hydrogenation of
oils. (5 Hrs.)
Soaps and Detergents: Introduction, raw materials, manufacture of soap, classification of
detergents, finishing of detergents. (5 Hrs.)
Carbon Technology: Introduction, classification of activated carbons, raw materials and
manufacture of activated carbons, classification of carbon fibres, precursors for carbon fibres,
manufacture of carbon fibres from polyacrylonitrile, manufacture of carbon black by furnace
black process, applications. (8 Hrs.)
Nanotechnolgy: Introduction, properties of nano particles like optical properties, reactivity,
synthesis of nano particles by RF plasma process.
Carbon nanotubes: Introduction, structure and properties of carbon nanotubes and fabrication of
carbon nanotubes, applications. (7 Hrs.)
Books Recommended:
1. Shreev, R.N. & Brink, J.A. : Chemical Process Industries, 5th Edition, McGraw Hill,
1987.
2. Austine, G.T. : Shreeves Chemicals Process Industries, 5th Edition, Mc
Graw Hill, 1984.
3. Dryden, C.E., Rao M.G. &
Silting, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., N. Delhi, 2008.
4. Pandey, G.N. : Chemical Technology, Volume-I, Lion Press, Kanpur.
5. Bansal, R.C. and Goyal, M. : Activated Carbon Adsorption, Taylor & Francis CRC
Group, N.Y., USA, 2005.
6. Bansal, R.C., Donnet, J.B. and
Stoeckli, F.
: Active Carbon, Marcel Dekker, N.Y.
7. Charles, P.P. and Frank, J.O. : Introduction to Nanotechnology, Wiley India Edition.
ICH 1.03 GENERAL ENGINEERING
Resultant of forces, moment of a force, moment of a couple, resultant of forces and couples,
equilibrium, analysis of trusses, centroids and moment of inertia of areas.
Simple stresses and simple strains, principle stresses and principle strains, shear force diagrams,
bending moment diagrams, torsion of shafts.
Fundamentals of thermodynamics, laws of thermodynamics, change of internal energy, change
of entropy, change of enthalpy and work done for various non-flow and flow processes,
introduction of carnot cycle, rankine cycle, refrigeration cycle, joule cycle, otto and diesel cycles.
Introduction to Electrical Engineering, simple networks analysis, electric motor, generator and
transformer. Application of ammeter, voltmeter, wattmeter, energy meter.
Books Recommended:
1. Meriam, J. L. : Statics, 5th Edition, John Wiley & Sons, 2002.
2. Singal, L. C. & Sharma, N. D. : Strength of Materials, 1st Edition, Modern
Publishers, 2002.
3. Ryder, G. H. : Strength of Materials, 3rd Edition, Mcmillan, 1992.
4. Nag, P.K. : Engineering Thermodynamics, 4th Edition, Mc Graw
Hill.
5. Threja, B. L. & Threja, A. K. : Electrical Technology, 3rd Edition (Vol I), Irja
Construction & Development Co. Private Ltd., 1992.
ICH 1.04 ANALYTICAL TECHNIQUES
1. Complexometric titrations: Complexes-formation constants; chelates – EDTA, Chelon
Effect, EDTA equilibria, effect of pH on EDTA equilibria, EDTA titration curves, endpoint –
detection and indicators; Importance of complexometric titrations. (3 Hrs.)
2. Solvent Extraction: Distribution law, extraction process, factors effecting extraction,
technique for extraction, quantitative treatment of solvent extraction equilibria, classification
of solvent extraction systems. Advantages and applications of solvent extraction. (4 Hrs.)
3. Chromatography: Introduction to chromatography, principles, classification of
chromatographic techniques, thin layer and paper chromatography – principle and technique.
Column Chromatography – Factors affecting column efficiency and applications. Gas –
liquid chromatography – theory, instrumentation and applications. HPLC – instrumentation,
method, column efficiency and applications. (12 Hrs.)
4. IR Spectroscopy: Origin, rigid rotor model, harmonic oscillator model, principle, modes of
vibrations of atoms in polyatomic molecules, instrumentation, selection rules, identification
of organic compounds on the basis of infrared spectra. (6 Hrs.)
5. UV-Vis Spectroscopy: Introduction, laws of absorption, origin of spectra, types of transitions,
selection rules, identification of organic compounds using UV-VIS spectroscopy. (5 Hrs.)
6. NMR: Principle, chemical shift, spin-spin coupling shift reagents, instrumentation, spectra
and molecular structure, identification of organic compounds on the basis of NMR. (5 Hrs.)
7. Thermoanalytical methods: Principle, classification of methods.
TGA – Instrumentation, factors affecting results and analysis of data. applications.
DTG – Instrumentation, analysis of data and applications.
DTA – Principle, Instrumentation and applications. (5 Hrs.)
Books Recommended:
1. Skoog, D. A. & West D. M. : Principles of Instrumental Analysis, 5th Edition, Saunders
College Publishers, USA.
2. Skoog, D. A. & West D. M. : Fundamentals of Analytical Chemistry, 7th Edition,
Saunders College Publishers, USA.
3. Willard, Meritt, Dean &
Settle
: Industrial Methods of Analysis, 7th Edition.
4. Galen W. Ewing. : Industrial Methods of Chemical Analysis, 5th Edition.
5. Silverstein R. M. &
Webster F.X.
: Spectrometric identification of Organic Compounds, 6th
Edition, John Wiley and Sons, Inc., USA.
SYLLABUS FOR ELECTIVE SUBJECTS (ICH 1.05 & ICH 2.05)
1. Oils and Fats Technology: Introduction, Properties and classification of oils, manufacture
of vegetable oils by expression and solvent extraction, processing of fats (alkali refining,
bleaching deodorization), fatty acids and glycerol, hydrogenation of oils, soap and its
manufacture, waxes.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
2. Paper Technology: Introduction, raw materials, pulping processes, sulphate pulp, soda
pulp, sulphite pulp, beating, refining, filling, sizing and colouring. Manufacture of paper,
calendaring, pollution problem, recovery of chemicals from spent liquor from sulphate and
sulphite process.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
3. Paints and Varnish Technology: Importance of paints & varnishes, inorganic and organic
pigments, natural and synthetic resins, thinners and solvents, dying, semi-dying, modified
synthetic oils, manufacture of paints and varnishes, formulation calculations, analysis and
testing.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
4. Sugar and Starch Technology:
Sugar: Introduction, manufacture of cane sugar, extraction of juice, purification of juice,
concentration, crystallization, drying and separation of crystals, refining of sugar, recovery
of sugar from molasses, baggase.
Starch: Introduction, manufacture of starches and corn syrup from corn, utilization of
molasses, baggase, corncob etc.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
5. Polymer Technology: Basic principles of polymer science, reaction kinetics techniques of
polymerization, fundamentals of polymer rheology and viscoelasticity.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw
Hill.
2. Gowariker, V. R., Viswanathan,
N. V. & Sreedhar, J.
: Polymer Science, 1st Edition, Wiley Eastern, New Delhi.
6. Polymer Processing: Principles of converting polymers into required shapes and forms,
various types of processing techniques – their description, machines involved and the
technological developments.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw
Hill.
2. Gowariker, V. R., Viswanathan,
N. V. & Sreedhar, J.
: Polymer Science, 1st Edition, Wiley Eastern, New
Delhi.
7. Fertilizers: Introduction, classification of fertilizers, mixed fertilizers, fixation of nitrogen,
manufacture of ammonia based fertilizers.
Phosphatic fertilizers: Raw materials, single superphosphate, triple superphosphate.
Potassic fertilizers: Manufacture of potassium chloride and potassium sulphate, compound
and complex fertilizers, bulk blended fertilizers, fluid fertilizers and pollution problems.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
8. Food Processing: Introduction to food processing industry, food preservation, additives,
different techniques of food preservation and processing for vegetables and fruits, different
types of unit operations involved in food processing, food packaging and aging problems.
Books Recommended:
1. Charm, S. C. : The Fundamentals of Food Engineering, A. V. I.
Publishing Co., 1971.
2. Warnel, J. N. : Principles of Diary Processings, Wilelesy Eastern, 1976.
9. Industrial Electrochemistry: Primary cells, secondary cells and fuel cells, semiconductors,
electropytic rectifiers, electroplating, electroforming, electro polishing, electro
refining and electro deposition, anodizing, electrochemical machining and grinding,
corrosion, electrochemical analysis, electrochemical preparation.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
10. Membrane Separation Processes: Fundamental, mechanism of membrane transport,
gaseous diffusion, separation in liquid phase, dialysis, reverse osmosis, ultra filtration
membrane, electromembrane processes. Transfer coefficients and their determination.
Engineering aspects of membrane separation and industrial applications.
Books Recommended:
1. H. Wang, Sun-Tak &
Kammermeyer, Karl.
: Membranes in Separation, Wiley Interscience.
2. Baum B. Halley, W. &
White, R. A.
: Membrane Separation Process, Elsevier Scientific Publication.
ICH 1.51 CHEMICAL ENGINEERING LAB – I
1. General study of pipe fittings, valves and other equipments in the Chemical Engineering Lab.
2. Pressure drop for flow through pipelines, valves and fittings.
3. Characteristic curves of centrifugal pump.
4. Flow measurement by the use of orifice meter, venturimeter, rotameter and pitot tube.
5. Flow over weirs and notches.
6. Pressure drop in fluidized beds.
7. Measurement of drag force, Stoke’s law, Filteration.
ICH 1.52 CHEMICAL TECHNOLOGY LAB. (ORGANIC)
1. Oils & Fats: Determination of Acid value, Iodine value, Saponification value.
2. Carbohydrates: Reducing and non reducing sugars by (i) Fehlings method (ii) Pavy’s
method.
3. Soaps: Determination of free and combined alkali, total fatty matter, moisture and
insolubles.
ICH 1.53 GENERAL ENGINEERING LAB.
Simple experiments related to mechanics, strength of materials and basic electrical engineering,
workshops and elementary drawing.
Books Recommended:
1. Chaudhary, H. R. : Practical Applied Mechanics, Mohindra Capital Pub.,
Chandigarh.
2. Bhatnagar, O. S. : Experiments in Electrical Engineering
ICH 1.54 ANALYTICAL TECHNIQUES LAB.
1. Determination of viscosity of NaCl/Sugar at different concentrations. Calculation of
partial molal volume of NaCl/Sugar at infinite dilution from density.
2. a) Verification of Lambert – Beer Law.
b) Colorimetric determination of the composition of Fe-Salicylate complex by Job’s
method of continuous variation.
3. a) Rf of organic compounds by TLC
b) Analysis of analgesic drugs (APC) by TLC.
c) Separation of o- & p-nitroaniline by column chromatography.
4. Determination of degree of dissociation and dissociation constant conductometrically.
5. Titration of week acid – strong base pH metrically and determination of the ionization
constant of weak Acid.
6. Complexometric titration (EDTA) for determination of Ca+2 and Zn+2 ions.
7. Thermal analysis of Pb (OOCCH3)4 & CaC2O4×H2O
Books Recommended:
1. Vogel : Practical Organic Chemistry, 3rd Edition, ELBS, 1989.
2. Vogel : Textbook of quantitative analysis, 5th Edition, ELBS, 1989.
3. Lavitt, B. P. : Findlay’s Practical Physical Chemistry edited by Lavitt, B. P.,
Longman group, 9th rev. Edition, 1978.
SYLLABUS FOR
MASTER OF SCIENCE (INDUSTRIAL CHEMISTRY)
SECOND SEMESTER
ICH 2.01 CHEMICAL ENGINEERING – II
1 Conduction: Steady state conduction in one dimensional system, general conduction
equation, effect of variable thermal conductivity, lagging on pipes, the critical thickness of
insulation on pipes. (5 Hrs.)
2 Convection: Free and forced convection, concept of heat transfer co-efficient, dimensionless
numbers in free and forced convection, Dimensional analysis, experimental determination of
heat transfer coefficient and common working correlations. (5 Hrs.)
3 Condensation and Boiling: Condensation heat transfer phenomenon, film condensation on
vertical plates and cylinders as well as on horizontal cylinders. Effects of non-condensable gases
and vapor velocity on condensation, pool boiling, forced convection boiling, working
correlations for pool boiling. (4 Hrs.)
4 Evaporation: Types of Evaporators, single and multiple effects, single effect calculations,
evaporator capacity, economy, effect of liquid head and boiling point elevation, methods of
feeding. (4 Hrs.)
5 Heat Exchangers: double pipe heat exchanger, 1,1 and 1,2 shell and tube heat exchangers,
overall heat transfer coefficients, heat exchanger mean temperature differences (4 Hrs.)
6 Mass transfer: Introduction to mass transfer and diffusion, molecular diffusion in gases and
liquids, diffusion coefficients for gases and liquids (3 Hrs.)
7 Mass transfer coefficients: types of mass transfer coefficients, mass transfer coefficients in
laminar flow, theories of mass transfer. (3 Hrs.)
8 Interphase mass transfer, concept of overall mass transfer coefficient. (3 Hrs.)
9 Gas absorption: material balance, concept of transfer units for the design of packed
absorbers. (4 Hrs.)
10 Distillation: differential distillation for binary systems, Fractionation of binary mixtures
using McCabe – Thiele method, minimum reflux ratio, minimum number of plates, plate
efficiencies. (5 Hrs.)
Books Recommended:
1. Mc Cabe, W.L., Smith, J.C. and
Harriot H.P.
: Unit Operations of Chemical Engineering, 7th Edition,
McGraw Hill,2005.
2. Holman, J.P. : Heat Transfer, McGraw Hill Publication Co.Ltd., New
Delhi, 9th Edition, 2008
3. Chapman, A.J. : Heat Transfer, Mc Millan Publishing Co., 4th Edition,
1984
4. Kern, D.Q. : Process heat Transfer, Tata McGraw Hill Publishing
Co., New Delhi, Edition 1997, 2006
5. Kreith, F. : Principles of Heat Transfer, Harper & Row Pub.,
London.
6. Geankoplis, C.J. : Transport Processes and Unit Operations, Prentice Hall
of India Pvt. Ltd., 3rd Edition, 1999.
7. Treybal, Robert E. : Mass Transfer Operations, 3rd Edition, McGraw-Hill,
1981.
ICH 2.02 CHEMICAL TECHNOLOGY (INORGANIC)
Chlor-Alkali Industry: Manufacture of Soda Ash by Solvay and modified Solvay process,
manufacture of caustic soda. (5 Hrs.)
Sulphuric Acid: Introduction, manufacture of sulphuric acid. (5 Hrs.)
Cement & Glass: Cement- types and manufacture of Portland cement. Glass- manufacture of
glass, application of special glasses. (5 Hrs.)
Ceramics- Refractories: Introduction, properties of ceramics, classification of refractories,
important steps involved in the manufacture of refractories. (5 Hrs.)
Industrial gases: Manufacture and uses of carbondioxide, oxygen, nitrogen and acetylene.
(6 Hrs.)
Paints: Introduction, classification of paints, manufacture of paints. (4 Hrs.)
Fertilizers: Nitrogeneous fertilizers- Manufacture of Ammonia, Nitric acid, Urea, CAN,
Ammonium Sulphate. Phosphatic fertilizers- superphosphate and triple superphosphate. Potassic
fertilizers- Potassium Chloride and Potassium Sulphate. (10 Hrs.)
Books Recommended:
1. Shreev, R.N. & Brink, J.A. : Chemical Process Industries, 5th Edition, McGraw Hill,
1987.
2. Austine, G.T. : Shreeves Chemicals Process Industries, 5th Edition, Mc
Graw Hill, 1984.
3. Dryden, C.E., Rao M.G. &
Silting, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., N. Delhi, 2008.
4. Pandey, G.N. : Chemical Technology, Volume-I, Lion Press, Kanpur.
5. Bansal, R.C. and Goyal, M. : Activated Carbon Adsorption, Taylor & Francis CRC
Group, N.Y., USA, 2005.
ICH 2.03 PROCESS INSTRUMENTATION
General Concept: Need and classification of measurements and instruments, Basic and auxiliary
functional elements of a measurement system. (1 Hr.)
Static and Dynamic Characteristics of Instruments:
Static Characteristics: Range and span, accuracy and static error, reproducibility and drift,
sensitivity and dead zone. (2 Hrs.)
Dynamic Characteristics: Speed of response and lag, fidelity and dynamic error, dead time.
Temperature measurement:
Thermal expansion methods – bimetallic thermometers, liquid-in-glass thermometer and filledin-
system thermometers.
Thermocouples, metal resistance thermometers and thermistors, optical and radiation
pyrometers, radiation receiving elements. (8 Hrs.)
Pressure measurement:
Use of manometers, Bourdon gauge, bellows type gauge. Vacuum measurement–Mcleod gauge,
thermoionic type ionization gauge, pirani vacuum gauge. Measurement of pressure in corrosive
fluids: Diaphragm seal, liquid seal and purge system. (8 Hrs.)
Liquid level measurement:
Direct measurement of liquid level –Float & tape liquid level gauge, float and shaft liquid level
unit, hydraulic remote transmission of liquid level.
Level measurement in open vessels: Bubbler system, diaphragm box system, air trap system.
Level measurement in pressure vessels – Differential pressure manometer, use of liquid seals
with a manometer, displacement float liquid level gauge. (6 Hrs.)
Measurement of viscosity, conductivity, humidity and pH. (6 Hrs.)
Density measurement – liquid level method, displacement meter and hydrometer. (2 Hrs.)
Measurement of weight – spring scale, pneumatic force meter and hydrostatic force meter.
(2 Hrs.)
Process Instrumentation–Recording instruments, indicating and signaling instruments, control
centre, transmission of instrument reading, instrumentation diagrams. (5 Hrs.)
Books Recommended:
TEXT BOOKS
1. Eckman, Donald P. : Industrial Instrumentation, CBS Publisher and Distributors, Indian
Reprint 2004.
2. Singh, S.K. : Industrial Instrumentation and Control, 2nd Edition, Tata McGraw – Hill, 2007.
REFERENCE BOOKS
1. Considine, D.N. : Process Instruments and Controls Handbook 2nd Edition, McGraw Hill,
1974.
2. Fribance, A.E. : Industrial Instrumentation Fundamentals, Tata McGraw – Hill
Publishing Co. Ltd., 1962.
3. Patranabis, D. : Principles of Industrial Instrumentation, 2nd Edition, Tata McGraw Hill
Publishing Co. Ltd., 1999.
ICH 2.04 ENGINEERING MATERIALS
1. Atomic Structure: Review of bonding in solids, structure –property-processing relationship.
(2 Hrs.)
2. Crystal Structure : Space lattice,crystal systems, Miller indices, effect of radius ratio on coordination,
structures of common metallic, polymeric, ceramic, amorphous and partly
crystalline materials. (6 Hrs.)
3. Imperfections in atomic arrangement: various defects in atomic arrangement, diffusion
phenomenon in solids, Fick’s first and second law of diffusion, solid solution, slip systems,
various methods of strengthening materials, Schmid’s law. (8 Hrs.)
4. Phase Diagrams and phase transformation: binary phase diagrams – Fe-Fe3C, Cu-Ni, Pb-Sn.
microstructure development, TTT diagrams, heat treatment processes-hot and cold working,
hardening and softening processes. (8 Hrs.)
5. Materials: Standards and specifications, unified alloy numbering system, ferrous metals and
alloys, non-ferrous metals and alloys; overview of ceramic, polymeric and composite
materials; Mechanical tests: standard test procedures for mechanical property determinationstrength,
toughness, fracture toughness, hardness, deformation, fatigue, creep etc. (8 Hrs.)
6. Corrosion: Types and mechanism of corrosion, factors influencing corrosion, combating
corrosion, selection of materials of construction for handling different chemicals. (8 Hrs.)
Books Recommended:
1. Askelland, Donald R. : The Science & Engineering of Materials, Saurabh
Printers Pvt. Ltd, Noida, 5th Edition, 2007.
2. Shackleford, J.F. : Introduction to Material Science for Engineers, Pearson
Education, 6th Edition, 2007.
3. Van-Vlack, L.H. : Elements of Material Science & Engineering, Addison
Wesley Publishing Co., 6th Edition, 1989.
4. Raghavan, V. : Material Science & Engineering, 5th Edition, Prentice
Hall of India Pvt. Ltd., New Delhi.
5. Callister Jr. William D. : Materials Science and Engineering- An Introduction,
Wiley.
6. Perry, Robert H. : Chemical Engineers Handbook, 7th Edition, McGraw
Hill.
ICH 2.51 CHEMICAL ENGINEERING LAB – II
General study of heat and mass transfer equipment in the Chemical Engineering Lab.
Determination of heat transfer co-efficient for different types of heat transfer equipment. Wilson
plots.
Correlation of instantaneous heat transfer coefficients with time, study of deposition of scale on a
heating surface.
Heat losses for insulated pipes
Duhring’s plot for solutions involving nonvolatile solutes.
Mass transfer coefficients for naphthalene-air system.
Drying rate curves for different wet materials.
Verification of Rayleigh’s equation for differential distillation. Flooding velocities in packed
columns. Determination of HETP for packed distillation columns.
ICH 2.52 CHEMICAL TECHNOLOGY LAB. (INORGANIC)
1. Fertilizers (i) Determination of N-P-K Values
(ii) Determination of micronutrients
2. Cement: Loss of ignition, silica, insolubles, estimation of Mg, Ca, Fe.
3. Water
ICH 2.53 MATERIALS LAB.
1. To study and calculate MFI (Property)
a) Conduct experiment of MFI as property and processing parameters.
b) Relation between molecular weight – structure and MFI.
2. To calculate and analyse the tensile strength of materials.
b) Films – idea of necking.
c) Polymers/Plastics.
3. To understand the processing techniques for various applications of materials
a) Compression moulding
b) Injection moulding
c) Film blow moulding – extrusion
d) Rotational moulding
4. To study and analyse tear/burst strength in packaging.
5. To analyse impact strength of materials especially polymers/composites
6. Processing of composites (glass fibre) and advanced materials
a) Glass fibre
b) Nano composites etc.
Books Recommended:
1. Shackleford, J.F. : Introduction to Material Science for Engineers, Pearson
Education, 6th Edition, 2007.
2. Raghavan, V. : Material Science & Engineering, 5th Edition, Prentice
Hall of India Pvt. Ltd., New Delhi.
3. Callister Jr. William D. : Materials Science and Engineering- An Introduction,
Wiley.
ICH 2.54 COMPUTERS APPLICATIONS
1. Introduction to computers, principles and operation of various types of computers,
concept of higher level language and compilers, line editing, compiling and running of a
small sample problems.
2. Use of internet.
3. C++ Fundamentals: Character set, identifiers, keywords, data types, constants, variables,
arrays, declarations, expressions, statements.
4. Operators and expressions.
5. Data input and output.
6. Writing of complete program and compiling.
7. Control statements.
8. Functions.
9. Arrays.
Books Recommended:
1. Lafore, R. : Object-Oriented Programming in Turbo C++, Galtotia
Publications Pvt. Ltd., New Delhi, 2001.
2. Hubbard, John R. : Schaum’s Outlines- Programming with C++, 2nd Edition, Tata
McGraw Hill Publishing Co. Ltd., New Delhi.
SYLLABUS FOR
MASTER OF SCIENCE (INDUSTRIAL CHEMISTRY)
THIRD SEMESTER
ICH 3.01 INDUSTRIAL POLUTION CONTROL
Environmental Pollution: Definition
Industrialization and energy-use as causes of Environmental Pollution.
Effects: Global warming, Acid rain, Ozone layer depletion, Photochemical smog.
Equitable use of resources for Sustainable lifestyle. (8 Hrs.)
Water pollution
Types of waste water, and sources of pollutants.
Determination of BOD and COD.
Basic concept of Industrial Wastewater Treatment:
• Primary treatment: Sedimentation, Flotation
• Secondary treatment: Activated Sludge process, Trickling Filters, Oxidation pond,
Rotating Biological Cyclone (RBC) and Anaerobic digester
• Tertiary treatment systems: Brief review about Coagulation and Filtration, Adsorption on
Activated carbon, Ion exchange, Reverse osmosis, Electrodialysis, Nitrogen and
Phosphorous removal. (12 Hrs.)
Air Pollution
Brief review of industrial pollution sources.
Classification and properties of major air pollutants, Effects of air pollution on human, plants and
materials.
Meteorology aspects of air pollution: lapse rate and stability conditions, characteristics of stack
plume.
Basic concept of Air pollution control methods:
• Particulate emission control: Gravitational settling chambers, Cyclone separators, Fabric
filters, Electrostatic precipitators, Wet scrubbers.
• Control of SOx and NOx gaseous emissions. (12 Hrs.)
Solid Waste Management
Types of solid wastes and sources.
Methods of solid waste management: Sanitary landfill, Incineration and Concept of Recycling.
(8 Hrs.)
Books Recommended:
1. Rao, C. S. : Environmental Pollution Control Engineering, New
Age Int. (P) Ltd. Publishers, 2006.
2. Rao, M.N. and Rao, H.V.N. : Air Pollution, Tata McGraw-Hill Publishing
Company Limited, New Delhi, 2003.
3. Zajic, J.E. : Water pollution, Marcel Dekker, Inc. New York,
1971.
4. Davis, M.L. and Cornwell, D.A. : Introduction to Environmental Engg. McGraw-Hill
International Editions, 1991.
ICH 3.02 CHEMICAL ENGINEERING – III
(a) Thermodynamics:
Brief review of the terms: state functions, types of systems, internal energy, heat and work
and reversible and irreversible processes. First Law of Thermodynamics and its Engineering
Applications i.e. constant volume processes, constant pressure processes, isothermal and
adiabatic processes, pumps, turbines, compressors, nozzles, heat exchangers, pitot tube,
venturimeter and orifice meter. Throttling Processes, Joule-Thomson Coefficient,
liquefication of gases.
Review of Second law of thermodynamics, entropy concept, entropy and lost work
calculations. Microscopic interpretation of entropy. Estimation of thermodynamic properties
by using graphs and tables.
Fugacity and its calculations. Dependence of fugacity of temperatures and pressure.
Solution behaviour of real liquids and solids. Activity and activity coefficients. Variation of
activity coefficient with temperature and composition.
(b) Reaction Kinetics:
Kinetics of homogeneous reactions, introduction to different types of reactors, analysis of
reversible, irreversible, series, parallel reaction schemes.
Books Recommended:
1. Smith, J.M. and Van Ness, H.C. : Introduction to Chemical Engg. Thermodynamics,
McGraw Hill Book Co., London.
2. Stiener, L.E. : Introduction to Chemical Thermodynamics, McGraw
Hill Book Co.
3. Levenspial, D. : Chemical Reaction Engineering, John Wiley.
4. Narayanan, K.V. : A Textbook of Chemical Engineering
Thermodynamics, PHI Learning Pvt. Ltd., 2004.
ICH 3.03 INDUSTRIAL MANAGEMENT
Process of decision making; elements in decision making; nature and frame work of planning;
Short and long range planning, policy formulation, organization structure and behaviour;
decentralization and delegation, line-staff relationship, motivation and morale, communication,
interpersonal and group behaviour, coordination and direction.
Purpose, processes and areas of control; control standards; control reports; budget as control device.
Economic planning and policy in India. Industrial policy, industrial development in India.
Position and problems of chemical industries in India.
Books Recommended:
1. Koontz & O’Donnel : Essentials of Management, New York, McGraw Hill
Publishing Company, 1990.
2. Terry, George, R. : Principles of Management, Homewood Richard, D.
Irwin INC., 1990.
3. Davar, R.S. : The Management Process, Bombay, Progressive
Corporation, 1980.
ICH 3.05 LITERATURE SURVEY, REPORT WRITING & SEMINAR
Forms of technical reports: aims and forms according to type of readership and extent of
circulation. Abstracts, extended abstracts. Tables, Graphs, Visual representation of data; slides,
microfilms, other techniques including those of audio-visual representation. Correct use of audio
equipment.
Research papers and their presentation and publication. Information retrieval direct and through
abstracts.
Practical training in writing and presentation of technical reports through audio visual means.
Techniques of effective public speaking, organized and imprompt discussions.
Preparation of a technical report on an assigned topic after survey of scientific, technical and
commercial literature, using card indexes, microfilms and other information retrieval methods.
Use of Computer Softwares for report writing.
Books Recommended:
1. Mildran, A.M. : Use of Engineering Literature, Butter Worths.
2. Sottle, R.T. : The Use of Chemical Literature, Butter, Worths.
3. Hoover, H. : Essentials for the Technical Writer, John Wiley.
4. Robertson, W.S. and Siddle,
W.D.
: Technical Writing and Presentation, Pergamon.
ICH 3.04 SYLLABUS FOR ELECTIVE SUBJECT (ELECTIVE-II)
1. Oils and Fats Technology: Introduction, Properties and classification of oils, manufacture
of vegetable oils by expression and solvent extraction, processing of fats (alkali refining,
bleaching deodorization), fatty acids and glycerol, hydrogenation of oils, soap and its
manufacture, waxes.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
2. Paper Technology: Introduction, raw materials, pulping processes, sulphate pulp, soda
pulp, sulphite pulp, beating, refining, filling, sizing and colouring. Manufacture of paper,
calendaring, pollution problem, recovery of chemicals from spent liquor from sulphate and
sulphite process.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
3. Paints and Varnish Technology: Importance of paints & varnishes, inorganic and organic
pigments, natural and synthetic resins, thinners and solvents, dying, semi-dying, modified
synthetic oils, manufacture of paints and varnishes, formulation calculations, analysis and
testing.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
4. Sugar and Starch Technology:
Sugar: Introduction, manufacture of cane sugar, extraction of juice, purification of juice,
concentration, crystallization, drying and separation of crystals, refining of sugar, recovery
of sugar from molasses, baggase.
Starch: Introduction, manufacture of starches and corn syrup from corn, utilization of
molasses, baggase, corncob etc.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
5. Polymer Technology: Basic principles of polymer science, reaction kinetics techniques of
polymerization, fundamentals of polymer rheology and viscoelasticity.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw
Hill.
2. Gowariker, V. R., Viswanathan,
N. V. & Sreedhar, J.
: Polymer Science, 1st Edition, Wiley Eastern, New Delhi.
6. Polymer Processing: Principles of converting polymers into required shapes and forms,
various types of processing techniques – their description, machines involved and the
technological developments.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw
Hill.
2. Gowariker, V. R., Viswanathan,
N. V. & Sreedhar, J.
: Polymer Science, 1st Edition, Wiley Eastern, New
Delhi.
7. Fertilizers: Introduction, classification of fertilizers, mixed fertilizers, fixation of nitrogen,
manufacture of ammonia based fertilizers.
Phosphatic fertilizers: Raw materials, single superphosphate, triple superphosphate.
Potassic fertilizers: Manufacture of potassium chloride and potassium sulphate, compound
and complex fertilizers, bulk blended fertilizers, fluid fertilizers and pollution problems.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
8. Food Processing: Introduction to food processing industry, food preservation, additives,
different techniques of food preservation and processing for vegetables and fruits, different
types of unit operations involved in food processing, food packaging and aging problems.
Books Recommended:
1. Charm, S. C. : The Fundamentals of Food Engineering, A. V. I.
Publishing Co., 1971.
2. Warnel, J. N. : Principles of Diary Processings, Wilelesy Eastern, 1976.
9. Industrial Electrochemistry: Primary cells, secondary cells and fuel cells, semiconductors,
electropytic rectifiers, electroplating, electroforming, electro polishing, electro
refining and electro deposition, anodizing, electrochemical machining and grinding,
corrosion, electrochemical analysis, electrochemical preparation.
Books Recommended:
1. Shreve, R. N. & Brink, J. A. : Chemical Process Industries, 5th Edition, McGraw Hill.
2. Dryden, C. E., Rao, M. G. &
Sitrig, M.
: Outlines of Chemical Technology, 3rd Edition, Affiliated
East West Press Pvt. Ltd., New Delhi.
3. Pandey, G. N. : A Textbook of Chemical Technology, Vol. I & II, 2nd
Edition, Vikas Publishing House Pvt. Ltd.
10. Membrane Separation Processes: Fundamental, mechanism of membrane transport,
gaseous diffusion, separation in liquid phase, dialysis, reverse osmosis, ultra filtration
membrane, electromembrane processes. Transfer coefficients and their determination.
Engineering aspects of membrane separation and industrial applications.
Books Recommended:
1. H. Wang, Sun-Tak &
Kammermeyer, Karl.
: Membranes in Separation, Wiley Interscience.
2. Baum B. Halley, W. &
White, R. A.
: Membrane Separation Process, Elsevier Scientific Publication.

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